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Benzaldehyde → (E)-2-(2-Benzylidenehydrazinyl)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Benzoic acid, 2-hydrazinyl-, hydrochloride (1:1) | HCID 104169 | — |
| 生成物 | (E)-2-(2-Benzylidenehydrazinyl)benzoic acid | HCID 9561044 | — |
反応手順
The title compound was prepared from 2-hydrazinobenzoic acid hydrochloride (1.89 g, 10.0 mmol) and benzaldehyde (1.06 g, 10.0 mmol) according to the procedure of Fischer, E. and co-workers described in Chem. Ber., 35, 1902, 2318 (2.4 g, quantitative yield). MS (DCI) m/z 241 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07902203B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-6d1024f6a29240f0b05f02af51dcb53d |
| 出典メモ | uspto-grants-2011_03 |