化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Hydroxide → O-2-trifluoromethylphenyl dimethylthiocarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| 反応物 | 2-Trifluoromethylphenol | HCID 67958 | — |
| 生成物 | O-2-trifluoromethylphenyl dimethylthiocarbamate | HCID 14795406 | 89% |
反応手順
If the procedure described in Preparation XI is followed starting from 3.95 g (24.3.10-3 mol) of 2-tri-fluoromethylphenol, 1.43 g (25.6.10-3 mol) of potassium hydroxide and 3.46 g (28.10-3 mol) of dimethylthiocarbamoyl chloride, 5.37 g (yield: 89%) of a yellow oil are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05246961 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-be2199f40d44415e9d6c4b76de61d7c9 |
| 出典メモ | uspto-grants-1993_09 |