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4-Iodo-1-methyl-1H-pyrazole-5-carboxylic acid → 4-(6-cyanopyridin-2-yl)-1-methyl-1H-pyrazole-5-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Iodo-1-methyl-1H-pyrazole-5-carboxylic acid | HCID 673687 | — |
| 反応物 | 6-Bromopyridine-2-carbonitrile | HCID 15100859 | — |
| 生成物 | 4-(6-cyanopyridin-2-yl)-1-methyl-1H-pyrazole-5-carboxylic acid | HCID 90383454 | 0.5% |
反応手順
Using 6-bromopicolinonitrile (0.73 g) and 4-iodo-1-methyl-1H-pyrazole-5-carboxylic acid (1 g), the title compound (4.7 mg) was obtained in the form of a colorless solid by the same method as that of (Example 3.22) <Step 1> or a method equivalent thereto.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09440970B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-4f71b1a0ad924789a5c437367e9bd3cf |
| 出典メモ | uspto-grants-2016_09 |