反応式
Br[C:2]1[C:9]([C:10]#[N:11])=[CH:8][C:7]([C:12]#[N:13])=[CH:6][C:3]=1[C:4]#[N:5].C[S-:15].[Na+]>>[C:4]([C:3]1[C:2]([SH:15])=[C:9]([CH:8]=[C:7]([C:12]#[N:13])[CH:6]=1)[C:10]#[N:11])#[N:5]参加物
3
実験手順
If the procedure described in Preparation LV is followed starting from 6 g (26.10-3 mol) of 2-bromo-3,5-dicyanobenzonitrile and 6 g (86.10-3 mol) of sodium thiomethylate, 6 g (quantitative yield) of the expected product are obtained in the form of an oil.
後処理
- customIf the procedure described in Preparation LV
出典と根拠
- ORDレコード
- ord-68057794265042cf843f66f80857944b
- 出典データセット
- uspto-grants-1993_09
- 特許番号
- US05246961
関連ノート
読み込み中…