化工社化工社 化学情報印刷レポート · 研究参考用
Eugenol → 4-Propylguaiacol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Eugenol | HCID 3314 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | 4-Propylguaiacol | HCID 17739 | — |
反応手順
Palladium-carbon (5 mass %, 54 mg) was added to a 2-propanol (2.5 mL) solution of eugenol (CAS No. 97-53-0, 500 mg) under an argon atmosphere. The resultant mixture was vigorously stirred at an external temperature of 50° C. under a hydrogen flow for about 4.5 hours. The reaction solution was filtered through Celite, and the filtrate was concentrated, to thereby obtain the title compound (447 mg) having the following physical properties.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07906549B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-4e043d5306dd4568b3fe3a8036310df1 |
| 出典メモ | uspto-grants-2011_03 |