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2,6-Dichlorophenol → N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dichlorophenol | HCID 6899 | — |
| 反応物 | 2-Chloro-N-(4-methylphenyl)acetamide | HCID 27967 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline | HCID 57952147 | — |
反応手順
Same procedure as example 6a starting from 2,6-dichlorophenol and 2-chloro-N-(4-methylphenyl)acetamide. At the end of the acetylation reaction the mixture was diluted with a small amount of toluene (0.2 part) to prevent solidification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07906677B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-af3bd9ab2c584e5988f942de2ef192e8 |
| 出典メモ | uspto-grants-2011_03 |