化工社化工社 化学情報印刷レポート · 研究参考用
3-Aminobiphenyl → N2,N4-Bis(3-phenylphenyl)-2,4-pyrimidinediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Aminobiphenyl | HCID 16717 | — |
| 反応物 | 2,4-Dichloro-5-fluoropyrimidine | HCID 250705 | — |
| 生成物 | N2,N4-Bis(3-phenylphenyl)-2,4-pyrimidinediamine | HCID 22060665 | — |
反応手順
In a like manner to the preparation of N2,N4-bis(3-hydroxyphenyl)-5-fluoro-2,4-pyrimidinediamine, 2,4-dichloro-5-fluoropyrimidine and 3-aminobiphenyl were reacted to provide N2,N4-Bis(3-phenylphenyl)-2,4-pyrimidinediamine. LCMS: purity: 98%; MS (m/e): 415 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07906644B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-35b7b1e192d74d11a2890789faf90add |
| 出典メモ | uspto-grants-2011_03 |