2-Fluorobenzoyl chloride → 2-fluoro-N-(4-fluoro-3-nitrophenyl)benzamide
反応式
[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH2:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[F:12][C:13]1[CH:21]=[CH:20][CH:19]=[CH:18][C:14]=1[C:15](Cl)=[O:16].S1C=CC=C1C(Cl)=O>>[F:12][C:13]1[CH:21]=[CH:20][CH:19]=[CH:18][C:14]=1[C:15]([NH:8][C:5]1[CH:6]=[CH:7][C:2]([F:1])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=1)=[O:16]参加物
4
実験手順
4-Fluoro-3-nitro-phenylamine was reacted with 2-fluorobenzoyl chloride according to the procedure of Example 256a substituting 2-fluorobenzoyl chloride for thiophene-2-carbonyl chloride to provide 2-fluoro-N-(4-fluoro-3-nitro-phenyl)-benzamide which was then reacted according to the procedures of Examples 256b and 256c to provide the title product.
出典と根拠
- ORDレコード
- ord-358a0388b12e4d92a1dde59affa1dea6
- 出典データセット
- uspto-grants-2011_03
- 特許番号
- US07910595B2
反応ノート
読み込み中…