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4-Fluoro-3-nitroaniline → N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluoro-3-nitroaniline | HCID 67768 | — |
| 反応物 | 2-Thiophenecarbonyl chloride | HCID 78928 | — |
| 反応物 | 3-Fluoro-5-(trifluoromethyl)benzoyl chloride | HCID 519364 | — |
| 生成物 | N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide | HCID 67040567 | — |
反応手順
4-Fluoro-3-nitro-phenylamine was reacted with 3-fluoro-5-trifluoromethyl-benzoyl chloride according to the procedure of Example 256a substituting 3-fluoro-5-trifluoromethyl-benzoyl chloride for thiophene-2-carbonyl chloride to provide N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide which was then reacted according to the procedures of Examples 256b and 256c to provide the title product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07910595B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-0c1e77ae6af04c2180c37813f7fe03c7 |
| 出典メモ | uspto-grants-2011_03 |