3-[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]propan-1-ol → HCID 66768815、化合物
反応式
N1[CH:5]=[N:4][C:3](SCCO)=N1.[C:10]1([C:16]([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[N:17]2[CH:21]=[N:20][C:19]([CH2:22][CH2:23][CH2:24][OH:25])=[N:18]2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:32]1([C:16]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)([C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)[N:17]2[CH:21]=[N:20][C:19]([CH2:22][CH2:23][CH2:24][O:25][C:5]3[CH:15]=[C:10]([C:16]#[N:17])[CH:11]=[CH:3][N:4]=3)=[N:18]2)[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1参加物
3
実験手順
By a method similar to that in Reference Example 17 and using, instead of 2-(1H-1,2,4-triazol-3-ylthio)ethanol, 3-[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]propan-1-ol obtained in Reference Example 26, the title compound was obtained as a white powder (314 mg, 88%).
後処理
- customobtained in Reference Example 26
出典と根拠
- ORDレコード
- ord-dcd2864414f345ba82e3089d2b047cde
- 出典データセット
- uspto-grants-2011_03
- 特許番号
- US07915267B2
反応ノート
読み込み中…