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Acrylic Acid → Isobornyl acrylate acrylic acid methyl acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Methyl Acrylate | HCID 7294 | — |
| 反応物 | 2-Methylundecane | HCID 23459 | — |
| 反応物 | 2,5-Dimethyl-2,5-bis(2-ethylhexanoylperoxy)hexane | HCID 114448 | — |
| 反応物 | Isobomyl acrylate | HCID 92004758 | — |
| 生成物 | Isobornyl acrylate acrylic acid methyl acrylate | HCID 131728765 | — |
反応手順
18 g of isobornyl acrylate, 71.1 g of methyl acrylate, 0.9 g of acrylic acid, 90 g of isododecane and 1.2 g of 2,5-bis(2-ethylhexanoylperoxy)-2,5-dimethylhexane were then introduced into the above mixture, still at 90° C. and over 1 hour.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07915347B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-526b6217ddeb4d10af672d4fdc719ab6 |
| 出典メモ | uspto-grants-2011_03 |