化工社化工社 化学情報印刷レポート · 研究参考用
Iodopyrazine → Methyl 5-methyl-2-(pyrazin-2-yl)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Iodopyrazine | HCID 642841 | — |
| 反応物 | Methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate | HCID 46856403 | — |
| 反応物 | Methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate | HCID 117727848 | — |
| 生成物 | Methyl 5-methyl-2-(pyrazin-2-yl)benzoate | HCID 117728053 | — |
反応手順
The title compound was synthesized following the same general protocol as described for methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate in Example A1, using methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate and using 2-iodopyrazine. ESI-MS (m/z): 229 [M+1]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09440982B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-49df807a707541b29b8c7e7fd0c9622e |
| 出典メモ | uspto-grants-2016_09 |