戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 60935作成日：2026年10月25日

2,4-Dichloropyrimidine → Methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoate

https://huagongshe.com/reaction/60935

反応式

関与物質

役割名称HCID仕込み量
反応物2,4-DichloropyrimidineHCID 77531—
反応物Methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoateHCID 46856403—
反応物Methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoateHCID 117727848—
生成物Methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoateHCID 117727617—

反応手順

The title compound was synthesized following the same general protocol as described for methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate in Example A1, using methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate and 2,4-dichloropyrimidine. ESI-MS (m/z): 263 [M+1]+.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09440982B2
出典データセットuspto-grants-2016_09
ORD IDord-5d81e4ba5f6343f09f530925509d1f00
出典メモuspto-grants-2016_09