反応式
[ClH:1].[CH3:2][C:3](=[CH:5][CH2:6][CH3:7])[CH3:4].[N:8]([O:10]CCC(C)C)=O>>[Cl:1][C:3]([CH3:4])([CH:5]([N:8]=[O:10])[CH2:6][CH3:7])[CH3:2]参加物
4
反応条件
- 温度
- -20 °C
実験手順
Dry hydrogen chloride gas was passed into a mixture of 2-methyl-2-pentene (20 g, 237 mmol) and iso-amyl nitrite (55.67 g, 475 mmol) cooled to -20° C. The reaction mixture was left to stir at 0° C. overnight and the precipitated material was then filtered off and washed with cold (-20° C.) ethanol (3×5 ml). The product was dried in a stream of air and was used without further purification, (13 g, 36%).
後処理
- waitThe reaction mixture was left
- filtrationthe precipitated material was then filtered off
- washwashed with cold (-20° C.) ethanol (3×5 ml)
- customThe product was dried in a stream of air
- customwas used without further purification, (13 g, 36%)
出典と根拠
- ORDレコード
- ord-05e94ea8f0d644f3b3c8be9d4ebb5bb0
- 出典データセット
- uspto-grants-1999_12
- 特許番号
- US05997843
関連ノート
読み込み中…