Morpholine → 3-Amino-3-morpholinoacrylonitrile

HRID 610040ノート

反応式

HRID 610040 の反応式
[C:1]([CH2:3][C:4](=[NH:8])OCC)#[N:2].[NH:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1>C(O)C>[NH2:8][C:4]([N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1)=[CH:3][C:1]#[N:2]

参加物

4

反応物 2

HCID 8083MorpholineHCID 256188Ethyl 2-cyanoethanecarboximidate

生成物 1

HCID 27636313-Amino-3-morpholinoacrylonitrile

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

In anhydrous ethanol (10 ml) was dissolved ethyl 2-cyanoacetimidate (1.0 g), followed by addition of morpholine (0.78 g). The mixture was stirred at room temperature for 4 hours, and the separated crystals were collected by filtration. This crystal crop was used as it was in the next reaction.

後処理

  1. filtrationthe separated crystals were collected by filtration
  2. customwas in the next reaction

出典と根拠

ORDレコード
ord-007f37c576bd446793605b8aa1a181ca
出典データセット
uspto-grants-1999_12
特許番号
US05998459

反応ノート

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