化工社化工社 化学情報印刷レポート · 研究参考用
3-Nitrobenzanilide → 3-Aminobenzanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Nitrobenzanilide | HCID 347755 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-Aminobenzanilide | HCID 84347 | 90.8% |
反応手順
10% Palladium on carbon (2.0 g) was added to a solution of 3-nitro-N-phenyl-benzamide (20 g, 83 mmol) in ethanol (225 mL) and the mixture was hydrogenated at 45 psi for 2 hours. The mixture was filtered through diatomaceous earth and concentrated to give a colorless solid (mp 118-120° C., 16 g, 90%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05998463 |
| 出典データセット | uspto-grants-1999_12 |
| ORD ID | ord-0de9ee7ba0624e6f89c88e7033107b63 |
| 出典メモ | uspto-grants-1999_12 |