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Chlorodimethylphenylsilane → n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorodimethylphenylsilane | HCID 13029 | — |
| 反応物 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 生成物 | n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide | HCID 54348567 | — |
反応手順
The title compound was prepared from the compound of Example e and 1.1 eq dimethylphenylsilyl chloride according to General Method A. Purification by HPLC with 1:9 ethyl acetate/hexanes gave 6.3 g of the desired product as a clear oil, a 91% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05998466 |
| 出典データセット | uspto-grants-1999_12 |
| ORD ID | ord-0a0d9b934c394363984f88c4575699c9 |
| 出典メモ | uspto-grants-1999_12 |