化工社化工社 化学情報印刷レポート · 研究参考用
2-chloro-N-ethylbenzamide → n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| 反応物 | Chloro(dimethyl)vinylsilane | HCID 519368 | — |
| 生成物 | n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide | HCID 18630374 | — |
反応手順
The title compound was prepared from the compound of Example f and 1.5 eq vinyldimethylsilyl chloride according to General Method C. Purification by HPLC with 1:4 ethyl acetate/hexanes gave 630 mg of the desired product as a white solid, a 9% yield. m.p. 86-89° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05998466 |
| 出典データセット | uspto-grants-1999_12 |
| ORD ID | ord-d8dad76c522c4ff1b01b78564ab1f2e6 |
| 出典メモ | uspto-grants-1999_12 |