Water → HCID 19600279、化合物
反応式
CS(O[CH2:6][CH2:7][C:8]1[CH:12]=[CH:11][O:10][CH:9]=1)(=O)=O.[C:13]1(=[O:23])[NH:17][C:16](=[O:18])[C:15]2=[CH:19][CH:20]=[CH:21][CH:22]=[C:14]12.[K].O>CN(C)C=O>[O:10]1[CH:11]=[CH:12][C:8]([CH2:7][CH2:6][N:17]2[C:16](=[O:18])[C:15]3=[CH:19][CH:20]=[CH:21][CH:22]=[C:14]3[C:13]2=[O:23])=[CH:9]1参加物
5
反応条件
- 温度
- 100 °C
実験手順
To a solution of the 2-(3-furyl)ethyl methanesulfonate in 500 ml of N,N-dimethylformamide, 14.2 g (76.8 mmol) of potassium phthalimide was added, followed by overnight stirring at 100° C. After cooling to room temperature, the reaction mixture was added to water while being stirred vigorously. The resulting precipitate was filtered, washed with water and dried to yield N-[2-(3-furyl)ethyl]phthalimide.
後処理
- temperatureAfter cooling to room temperature
- stirringwhile being stirred vigorously
- filtrationThe resulting precipitate was filtered
- washwashed with water
- customdried
出典と根拠
- ORDレコード
- ord-ee6a041d586442d5b95af9b36bd631a6
- 出典データセット
- uspto-grants-1999_12
- 特許番号
- US05998433
反応ノート
読み込み中…