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HRID 611175作成日:2026年10月27日

Hydrochloric Acid → 1-(2-diethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-6-phenylhexan-1-one hydrochloride

https://huagongshe.com/reaction/611175

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrochloric AcidHCID 313—
反応物1-(2-diethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-6-phenylhexan-1-oneHCID 19600161—
溶媒MethanolHCID 887—
生成物1-(2-diethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-6-phenylhexan-1-one hydrochlorideHCID 19600278—

反応手順

1-(2-Diethylaminomethyl-6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-6-phenylhexan-1-one 0.209 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. After this mixture was concentrated, diethyl ether was added; the resulting solid was filtered and washed with diethyl ether to yield the desired product.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05998433
出典データセットuspto-grants-1999_12
ORD IDord-25c02bd397284bc1bb5b1ce461bbeba8
出典メモuspto-grants-1999_12