2-Iodo-3-methylbenzoic acid → 3-Methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid
反応式
C[C:2]1[CH:3]=[CH:4][C:5]([N:11]2[N:15]=[CH:14][CH:13]=[N:12]2)=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8].[CH3:16]C1C(I)=C(C=CC=1)C(O)=O.N1C=CN=N1>>[CH3:16][C:4]1[C:5]([N:11]2[N:12]=[CH:13][CH:14]=[N:15]2)=[C:6]([CH:10]=[CH:2][CH:3]=1)[C:7]([OH:9])=[O:8]参加物
4
実験手順
The title compound was prepared following the same general protocol as described for 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid in Example A11 using 3-methyl-2-iodobenzoic acid and 1,2,3-triazole. ESI-MS (m/z): 204 [M+1]+.
出典と根拠
- ORDレコード
- ord-eb4a4c27b5be4571965460b51dd9bd19
- 出典データセット
- uspto-grants-2016_09
- 特許番号
- US09440982B2
反応ノート
読み込み中…