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Potassium Carbonate → Dimethyl 4-(4-methoxybenzyloxy)phthalate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| 反応物 | Dimethyl 4-hydroxyphthalate | HCID 89726 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Dimethyl 4-(4-methoxybenzyloxy)phthalate | HCID 19595683 | — |
反応手順
1 eq. of dimethyl 4-hydroxyphthalate, 1.1 eq. of potassium carbonate and 1.1 eq. of 4-methoxybenzyl chloride were stirred in DMF at RT. After 4 days, the mixture was worked up according to a standard procedure. Dimethyl 4-(4-methoxybenzyloxy)phthalate was isolated as a colorless oil. MS: 331 ((M+1)+)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06005010 |
| 出典データセット | uspto-grants-1999_12 |
| ORD ID | ord-6aa64a686a13461fbdec1ab546ad0f32 |
| 出典メモ | uspto-grants-1999_12 |