関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 反応物 | N-Isopropylacrylamide | HCID 16637 | — |
| 反応物 | Methacrylamidopropyltrimethylammonium chloride | HCID 106428 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | MAPTAC N-Isopropylacrylamide HEMA | HCID 131721520 | — |
反応手順
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 8.9 g of a 50% aqueous solution of N-(3-trimethylammoniopropyl)methacrylamide chloride, 15.3 g of N-iso-propylacrylamide, and 4.4 g of 2-hydroxyethylmethacrylate. The solution was purged with nitrogen for 1 hour and 0.5 g of AIBN was added. The mixture was purged for 15 min until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06007803 |
|---|
| 出典データセット | uspto-grants-1999_12 |
|---|
| ORD ID | ord-95ea9e826a8d42838452997224629e81 |
|---|
| 出典メモ | uspto-grants-1999_12 |
|---|
