Methyl 3-(chlorosulfonyl)propanoate → Methyl 3-[2-[2-(4-methylphenyl)ethoxy]ethylaminosulphonyl]propanoate
反応式
Cl.[CH3:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][O:11][CH2:12][CH2:13][NH2:14])=[CH:5][CH:4]=1.Cl[S:16]([CH2:19][CH2:20][C:21]([O:23][CH3:24])=[O:22])(=[O:18])=[O:17]>ClCCl>[CH3:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][O:11][CH2:12][CH2:13][NH:14][S:16]([CH2:19][CH2:20][C:21]([O:23][CH3:24])=[O:22])(=[O:18])=[O:17])=[CH:7][CH:8]=1参加物
4
実験手順
The subtitle compound (2.49 g) was prepared according to the procedure in example 5 part d using 2-[2-(4-methylphenyl)ethoxy]ethanamine hydrochloride (3.5 g) triethylamine 4.74 ml) methyl 3-(chlorosulphonyl)propanoate (3.08 g), and dichloromethane (80 ml).
出典と根拠
- ORDレコード
- ord-0ec0131e5d904d679d7cc6af6447f5ea
- 出典データセット
- uspto-grants-1999_12
- 特許番号
- US06008365
反応ノート
読み込み中…