3-[2-(3-Formylphenoxy)ethoxy]benzaldehyde → HCID 178478834、化合物
反応式
[CH2:1]([CH2:11][O:12][C:13]1[CH:14]=[C:15]([CH:18]=[CH:19][CH:20]=1)[CH:16]=O)[O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH:6]=O.[C:21]([NH:24][NH2:25])([NH2:23])=[NH:22].[ClH:26]>C(O)C.Cl.Cl.NNC(N)=N>[ClH:26].[ClH:26].[C:21]([NH:24][N:25]=[CH:6][C:5]1[CH:8]=[CH:9][CH:10]=[C:3]([O:2][CH2:1][CH2:11][O:12][C:13]2[CH:14]=[C:15]([CH:18]=[CH:19][CH:20]=2)[CH:16]=[N:25][NH:24][C:21](=[NH:22])[NH2:23])[CH:4]=1)(=[NH:23])[NH2:22]参加物
5
実験手順
3,3'-(ethylenedioxy)dibenzaldehyde (1.08 g), aminoguanidine hydrochloride (1.105 g), and aminoguanidine dihydrochloride (0.005 g) were heated in 96% ethanol (6.25 mL) for 18 hr under nitrogen. Cooling and filtration gave 1.428 g of 3,3'-(ethylenedioxy)dibenzaldehyde bis(amidinohydrazone) dihydrochloride, mp 264-6° C.