関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanolamine | HCID 700 | — |
| 反応物 | Ethyl Lactate | HCID 7344 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-(2-hydroxyethyl)lactamide | HCID 95457 | — |
反応手順
A mixture of 70.8 gm (0.6 mole) of ethyl lactate and 36.6 gm (0.6 mole) of ethanolamine were stirred together at 60° C. for 16 hours, and the ethanol formed was subsequently distilled off under reduced pressure. 71 gm (89% of theory) of light yellow, viscous N-(2-hydroxyethyl)-lactic acid amide of refractive index (nD20) 1.4850 were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04143159 |
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| 出典データセット | uspto-grants-1979_03 |
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| ORD ID | ord-de0158ec03774a6aa1076a2cdc2f7e1e |
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| 出典メモ | uspto-grants-1979_03 |
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