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Glyceraldehyde → 4-(n-Hexadecylamino)benzoyl glyceraldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glyceraldehyde | HCID 751 | — |
| 反応物 | Chloroform | HCID 6212 | — |
| 反応物 | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| 触媒 | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-(n-Hexadecylamino)benzoyl glyceraldehyde | HCID 21326953 | — |
反応手順
To a mixture of 3.6 g. of glyceraldehyde and 2.44 g. of 4-dimethylaminopyridine in an ice-bath is added 4.16 g. of 4-(n-hexadecylamino)benzoyl chloride hydrochloride. After 4 hours at room temperature, chloroform and water are added. The chloroform extract is chromatographed quickly and evaporated in vacuo to yield 4-(n-hexadecylamino)benzoyl glyceraldehyde.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04146546 |
| 出典データセット | uspto-grants-1979_03 |
| ORD ID | ord-66fef1a1db6948c9940bcde96e59a27b |
| 出典メモ | uspto-grants-1979_03 |