化工社化工社 化学情報印刷レポート · 研究参考用
Bis(2-ethylhexyl)amine → 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bis(2-ethylhexyl)amine | HCID 7791 | — |
| 反応物 | Chloro(phenyl)acetyl chloride | HCID 102902 | — |
| 生成物 | 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide | HCID 118059549 | 96% |
反応手順
Step A is conducted starting from 2,2′-diethylhexylamine and α-chlorophenylacetyl chloride and leads to 2-chloro-N,N-bis(2-ethylhexyl)-2-phenyl-acetamide (Yield: 96%) for which the characterisations by 1H and 13C NMR are given below:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09441285B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-0e9e4199149b43188a2b7b866cc8e30c |
| 出典メモ | uspto-grants-2016_09 |