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Hydrochloric Acid → Acetylphenylstearic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 反応物 | 2-Phenyloctadecanoic acid | HCID 22015237 | — |
| 反応物 | HCID 131714100 | HCID 131714100 | — |
| 溶媒 | Carbon Tetrachloride | HCID 5943 | — |
| 生成物 | Acetylphenylstearic acid | HCID 70477797 | — |
反応手順
A 500 ml reaction vessel was charged with 200 mls freshly distilled carbon tetrachloride and the CCl4 was cooled to 0°-5° C. Aluminum chloride (0.33 moles) was added, via Gooch tubing, to the CCl4 over a period of 20 minutes. Acetyl chloride (0.35 mol) was added to an addition funnel and charged to the CCl4 -AlCl3 mixture. Phenylstearic acid (0.125 moles) was then slowly added to the reaction mixture from an addition funnel while maintaining the temperature of the reaction mixture at 0°-5° C. The temperature was maintained at 0°-5° C. for one hour and at room temperature for an additional two hours. The evolution of HCl was observed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04499013 |
| 出典データセット | uspto-grants-1985_02 |
| ORD ID | ord-81c1187f66ae4a17949542ab91d3be67 |
| 出典メモ | uspto-grants-1985_02 |