関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Phosphorus tribromide | HCID 24614 | — |
| 反応物 | 2-Indanol | HCID 77936 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | 2-bromo-2,3-dihydro-1H-indene | HCID 10965463 | — |
反応手順
To 80 gms of 2-indanol in 200 ml of chloroform was added 12 ml of pyridine. The solution was cooled to 0° C. with an ice bath, and 64 ml of phosphorous tribromide slowly added over 30 minutes. The ice bath was removed, and the solution was refluxed for 1 hour, and let stand overnight.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04500713 |
|---|
| 出典データセット | uspto-grants-1985_02 |
|---|
| ORD ID | ord-b54c7438a02d4835acdf095dca28bab3 |
|---|
| 出典メモ | uspto-grants-1985_02 |
|---|
