Ammonia → N,N-Dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)pentanamide

HRID 615967ノート

反応式

HRID 615967 の反応式
N.[CH3:2][C:3]1[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5][N:6]([CH:8]([CH2:12][CH2:13][CH3:14])[C:9](O)=[O:10])[CH:7]=1.C[CH:22]([N:26]1[CH:30]=C(C)C(C2C=CC=CC=2)=N1)C(O)=O>>[CH3:22][N:26]([CH3:30])[C:9](=[O:10])[CH:8]([CH2:12][CH2:13][CH3:14])[N:6]1[CH:7]=[C:3]([CH3:2])[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5]1

参加物

4

反応物 3

HCID 222AmmoniaHCID 20370468alpha,4-Dimethyl-3-phenyl-1H-pyrazole-1-acetic acidHCID 53897824HCID 53897824、化合物

生成物 1

HCID 20370492N,N-Dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)pentanamide

実験手順

Following the procedure of Example 68, but substituting dimethylamine for aqueous ammonia and 4-methyl-3-phenyl-α-propylpyrazole-1-acetic acid for α,4-dimethyl-3-phenylpyrazole-1-acetic acid, there was obtained N,N,4-trimethyl-3-phenyl-α-propylpyrazole-1-acetamide having a melting point of 84°-86° C.

出典と根拠

ORDレコード
ord-647857792c6646069624294dae13db14
出典データセット
uspto-grants-1978_02
特許番号
US04072498

反応ノート

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