Ammonia → HCID 20370577、化合物

反応式

N.[CH3:2][C:3]1[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5][N:6]([CH:8]([CH2:12][CH2:13][CH3:14])[C:9]([OH:11])=O)[CH:7]=1.[CH3:21][CH:22]([N:26]1[CH:30]=[C:29](C)C(C2C=CC=CC=2)=N1)C(O)=O>>[CH2:22]([N:26]([CH2:30][CH3:29])[C:9](=[O:11])[CH:8]([CH2:12][CH2:13][CH3:14])[N:6]1[CH:7]=[C:3]([CH3:2])[C:4]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[N:5]1)[CH3:21]

参加物

反応物 3

HCID 222Ammonia

HCID 20370468alpha,4-Dimethyl-3-phenyl-1H-pyrazole-1-acetic acid

HCID 53897824HCID 53897824、化合物

生成物 1

HCID 20370577HCID 20370577、化合物

実験手順

Following the procedure of Example 68, but substituting diethylamine for aqueous ammonia and 4-methyl-3-phenyl-α-propylpyrazole-1-acetic acid for α,4-dimethyl-3-phenylpyrazole-1-acetic acid, there was obtained N,N-diethyl-4-methyl-3-phenyl-α-propylpyrazole-1acetamide having a melting point of 65°-67° C.

出典と根拠

ORDレコード: ord-2a16a8a494414b258f742427a92eedee
出典データセット: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04072498

反応ノート

読み込み中…