Ammonia → HCID 20370606、化合物

反応式

[CH3:1][CH:2]([N:6]1[CH:10]=[C:9](C)[C:8]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[N:7]1)[C:3]([OH:5])=O.[CH2:18]([NH:20][CH2:21][CH3:22])[CH3:19].N>>[CH2:18]([N:20]([CH2:21][CH3:22])[C:3](=[O:5])[CH:2]([CH3:1])[N:6]1[CH:10]=[CH:9][C:8]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[N:7]1)[CH3:19]

参加物

反応物 3

HCID 222Ammonia

HCID 8021Diethylamine

HCID 20370468alpha,4-Dimethyl-3-phenyl-1H-pyrazole-1-acetic acid

生成物 1

HCID 20370606HCID 20370606、化合物

実験手順

Following the procedure of Example 68, but substituting α-methyl-3-phenylpyrazole-1-acetic acid for α,4-dimethyl-3-phenylpyrazole-1-acetic acid, and diethylamine for aqueous ammonia there was obtained N,N-diethyl-α-methyl-3-phenylpyrazole-1-acetamide having a boiling point of 178°/0.2 mm.

出典と根拠

ORDレコード: ord-d787b9600f754e28a114c80ad8925609
出典データセット: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04072498

反応ノート

読み込み中…