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3,5-Dimethylbenzene-1,2-diol → 2,6-Dimethylhydroquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dimethylbenzene-1,2-diol | HCID 17737 | — |
| 反応物 | Sodium bisulfate monohydrate | HCID 23673662 | — |
| 生成物 | 2,6-Dimethylhydroquinone | HCID 69560 | — |
反応手順
By following the same manner as in Example 56 except that 0.013 g. of sodium hydrogen sulfate monohydrate (NaHSO4.H2O) was used, 3.42 g. (24.8 m.moles) of 3,5-dimethylcatechol and 1.66 g. (12.0 m.moles) of 2,6-dimethylhydroquinone were obtained. The yield of dihydric alkylphenols was 87.4%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04072722 |
| 出典データセット | uspto-grants-1978_02 |
| ORD ID | ord-e8eb4463ed3a4d5b87ea66d84ee73561 |
| 出典メモ | uspto-grants-1978_02 |