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Sulfuric Acid → 2,6-Dimethylhydroquinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 3,5-Dimethylbenzene-1,2-diol | HCID 17737 | — |
| 生成物 | 2,6-Dimethylhydroquinone | HCID 69560 | — |
反応手順
By following in the same manner as in Example 56 except that 0.11 g. of strong acidic sulfontype ion exchange resin Amberlyst 15 (manufactured by Rohm and Hass Co.) was used instead of sulfuric acid, 2.55 g. (18.5 m.moles) of 3,5-dimethylcatechol and 1.26 g. (9.1 m.moles) of 2,6-dimethylhydroquinone were obtained. The yield of dihydric alkylphenols was 65.6%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04072722 |
| 出典データセット | uspto-grants-1978_02 |
| ORD ID | ord-6552ffe34cc045bab2d0743ec152c946 |
| 出典メモ | uspto-grants-1978_02 |