関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Ethylhexanoyl chloride | HCID 79103 | — |
| 反応物 | 2,5-Dimethylhexane 2,5-dihydroperoxide | HCID 520470 | — |
| 生成物 | 2,5-Dimethyl-2,5-bis(2-ethylhexanoylperoxy)hexane | HCID 114448 | — |
反応手順
Sodium hydroxide (25% aqueous solution), 2-ethylhexanoyl chloride (93%), 2,5-dimethyl-2,5-dihydroperoxyhexane (70%) are introduced into the mixing reactor (21) along with an aliphatic organic solvent (hexane, heptane etc.) at the rate of 51 lbs/hr, 31 lbs/hr and 38 lbs/hr respectively. The temperature in the reaction zone 21 is maintained at about 30° C and that in the after reaction zone 22 at about 20° C. The product 2,5-dimethyl-2,5-di(2-ethylhexanoylperoxy)hexane is obtained at the rate of about 50 lbs/hr.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04075236 |
|---|
| 出典データセット | uspto-grants-1978_02 |
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| ORD ID | ord-6ebc1d152e3f490aa29dc68de9327810 |
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| 出典メモ | uspto-grants-1978_02 |
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