関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | 5-Chlorothiophene-2-sulfonyl chloride | HCID 2733925 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | 5-Chloro-4-nitrothiophene-2-sulfonyl chloride | HCID 2735783 | — |
反応手順
A 32.5-g (0.15 mol) sample of 5-chloro-2-thienylsulfonyl chloride was added in small portions to a stirred solution of 150 ml concentrated nitric acid and 150 ml concentrated sulfuric acid. After the addition was completed, the reaction mixture was stirred at about 25° C overnight. The reaction mixture was then diluted with ice water and filtered to give the 5-chloro-4-nitro-2-thienylsulfonyl chloride product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04075347 |
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| 出典データセット | uspto-grants-1978_02 |
|---|
| ORD ID | ord-5f85466c5728470e8f71830812e4e1aa |
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| 出典メモ | uspto-grants-1978_02 |
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