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Hydrogen Bromide → Silver bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | Lauric Acid | HCID 3893 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Silver Nitrate | HCID 24470 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Silver bromide | HCID 66199 | — |
| 生成物 | Silver laurate | HCID 9904644 | — |
反応手順
One liter of an aqueous solution of 20 g of sodium hydroxide was mixed with 2 liters of toluene having dissolved therein 120 g of lauric acid, and the mixture was emulsified using a high speed rotary stirrer. To the emulsion, 500 ml of a 0.4% by weight aqueous solution of hydrobromic acid was added, and the mixture was again emulsified. To the resulting emulsion, 500 ml of an aqueous solution of 85 g of silver nitrate was added to form silver laurate and silver bromide simultaneously. The toluene phase containing the silver nitrate and the silver bromide was separated from the aqueous phase, and dispersed in 2.4 Kg of a 15% by weight isopropanol solution of polyvinyl butyral using a high speed rotary stirrer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04076534 |
| 出典データセット | uspto-grants-1978_02 |
| ORD ID | ord-295ec46675b645f9b71b64ae2c3039dd |
| 出典メモ | uspto-grants-1978_02 |