化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Ethyl 3-methylbenzimidate hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 3-Tolunitrile | HCID 12104 | — |
| 生成物 | Ethyl 3-methylbenzimidate hydrochloride | HCID 21938086 | — |
反応手順
Ethyl 3-methylbenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, m-tolunitrile (25.2 g, 0.215 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 41.7 g (97%) of the target compound as colorless crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05948785 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-472e9956c224470ca9bd5bd552bcd52d |
| 出典メモ | uspto-grants-1999_09 |