化工社化工社 化学情報印刷レポート · 研究参考用
3',4',5'-Trimethoxyacetophenone → (E)-3-(5-Fluoroindol-3-yl)-1-(3,4,5-trimethoxyphenyl)-2-propen-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3',4',5'-Trimethoxyacetophenone | HCID 14345 | — |
| 反応物 | 5-fluoro-1H-indole-3-carbaldehyde | HCID 259089 | — |
| 生成物 | (E)-3-(5-Fluoroindol-3-yl)-1-(3,4,5-trimethoxyphenyl)-2-propen-1-one | HCID 21850276 | 59.2% |
反応手順
Substantially the same procedure as in Example 12 was repeated using 3',4',5'-trimethoxyacetophenone (2.1 g) and 5-fluoroindole-3-carboxaldehyde (1.63 g) to give Compound 29 (2.1 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952355 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-ba16b9df620e4d88a82381f067c78d28 |
| 出典メモ | uspto-grants-1999_09 |