(4-Nitrophenyl)hydrazine → 8-Methoxy-6,6-dimethyl-2-nitro-6,11-dihydro-5H-benzo[b]carbazole

HRID 61817

反応式

HRID 61817 の反応式
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][C:9](=O)[C:10]2([CH3:14])[CH3:13])=[CH:5][CH:4]=1.[N+:16]([C:19]1[CH:24]=[CH:23][C:22]([NH:25]N)=[CH:21][CH:20]=1)([O-:18])=[O:17]>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[CH2:7][C:8]3[C:23]4[C:22](=[CH:21][CH:20]=[C:19]([N+:16]([O-:18])=[O:17])[CH:24]=4)[NH:25][C:9]=3[C:10]([CH3:14])([CH3:13])[C:11]=2[CH:12]=1

参加物

3

反応物 2

HCID 3310889(4-Nitrophenyl)hydrazineHCID 130110077-Methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one

生成物 1

HCID 668342128-Methoxy-6,6-dimethyl-2-nitro-6,11-dihydro-5H-benzo[b]carbazole

実験手順

Under the same conditions as the method for synthesizing Compound A3-1, the title compound was prepared from Compound A2 and 4-nitrophenylhydrazine.

後処理

  1. customUnder the same conditions as the method for synthesizing Compound A3-1

出典と根拠

ORDレコード
ord-4601063574764f859c47f42e2215cb2c
出典データセット
uspto-grants-2016_09
特許番号
US09440922B2

関連ノート

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