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Dimethylformamide → 7-Methoxyheptanoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | 7-Bromoheptanoic acid | HCID 121723 | — |
| 生成物 | 7-Methoxyheptanoic Acid | HCID 15409528 | — |
反応手順
The title compound was prepared by the method of Example 1 using 7-bromoheptanoic acid (50 g, 239 mmol) instead of 12-bromoundecanoic acid and dimethylformamide (300 mL) instead of methanol as the solvent. Concentration afforded the title compound (30 g) as a pale yellow liquid and the structure verified by NMR.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952377 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-9f269605ad5e4ef8828b7ab218008c5e |
| 出典メモ | uspto-grants-1999_09 |