化工社化工社 化学情報印刷レポート · 研究参考用
1-(Chloromethoxy)-2-methoxyethane → Methyl 4-[7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthyl]benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(Chloromethoxy)-2-methoxyethane | HCID 77590 | — |
| 反応物 | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| 生成物 | Methyl 4-[7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthyl]benzoate | HCID 70230892 | 55% |
反応手順
Following the procedure of Example 1(a), but reacting 980 mg (2.4 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 330 μl (28.6 mmol) of methoxyethoxymethyl chloride, 650 mg (55%) of the expected compound were obtained in the form of an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952382 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-937de1c627fe4383bb98791d8aac73d0 |
| 出典メモ | uspto-grants-1999_09 |