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6-Bromohexanamide → Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Bromohexanamide | HCID 321974 | — |
| 反応物 | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| 生成物 | Methyl 4-[7-(1-adamantyl)-6-carbonylpentyloxy-2-naphthyl]benzoate | HCID 21850744 | 66% |
反応手順
Following the procedure of Example 12(a), but reacting 640 mg (1.55 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 450 mg (2.32 mmol) of 6-bromohexanamide, 520 mg (65%) of the expected compound were obtained, which compound had a melting point of 209°-10° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05952382 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-55058d0f2c0a4a00b492fdcfcf9a0cb5 |
| 出典メモ | uspto-grants-1999_09 |