化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → Z-Gln-ome
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Sulfuryl chloride | HCID 24648 | — |
| 反応物 | L-Glutamine, N2-[(phenylmethoxy)carbonyl]- | HCID 75855 | — |
| 生成物 | Z-Gln-ome | HCID 7020255 | — |
反応手順
Sulphuryl chloride (1 g) was added to a stirred mixture of N-benzyloxycarbonyl-L-glutamine (100 g) and methanol (1200 ml) and the mixture was stirred at ambient temperature for 24 hours. The mixture was evaporated to give N-benzyloxycarbonyl-L-glutamine methyl ester (105 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05955463 |
| 出典データセット | uspto-grants-1999_09 |
| ORD ID | ord-7c388e813ccc4a57ab2a1f330e68813f |
| 出典メモ | uspto-grants-1999_09 |