Benzyl Bromide → HCID 14155410、化合物

反応式

[NH2:1][C:2]1[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][OH:5].[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:5][CH2:4][C:3]1[CH:6]=[CH:7][CH:8]=[C:9]([Cl:10])[C:2]=1[NH2:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

参加物

反応物 2

HCID 7498Benzyl Bromide

HCID 14155407(2-Amino-3-chlorophenyl)methanol

生成物 1

HCID 14155410HCID 14155410、化合物

実験手順

This material was prepared from 2-amino-3-chlorobenzyl alcohol and benzyl bromide by the general procedure outlined in Example 98. The product was purified by Kugelrohr distillation to yield an oil, b.p. 118°-125° C. (0.1 mm). The product was characterized by IR and 1H NMR spectroscopy.

後処理

distillationThe product was purified by Kugelrohr distillation
customto yield an oil, b.p. 118°-125° C. (0.1 mm)

出典と根拠

ORDレコード: ord-ff50a2dedae3455b818124a0c95d3937
出典データセット: uspto-grants-1989_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04818273

反応ノート

読み込み中…

参加物