化工社化工社 化学情報印刷レポート · 研究参考用
Methyl iodide → 1,1-Dimethyl-3-hydroxypiperidinium Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | Dichloromethane | HCID 6344 | — |
| 反応物 | 3-Piperidinol, 1-methyl- | HCID 98016 | — |
| 生成物 | 1,1-Dimethyl-3-hydroxypiperidinium Chloride | HCID 21247485 | — |
反応手順
This compound was prepared by the procedure described for 2-[4-(N,N,N-trimethylammonium)phenyl]ethanol chloride. Typical reagent levels were as follows: 3-hydroxy-1-methylpiperidine (21.7 g, 0.188 mol), iodomethane (40.0 g, 0.280 mol) and methylene chloride (50 ml).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04818426 |
| 出典データセット | uspto-grants-1989_04 |
| ORD ID | ord-0f06b4d483da430bbc56756d0f569330 |
| 出典メモ | uspto-grants-1989_04 |