化工社化工社 化学情報印刷レポート · 研究参考用
Acrylamide → Lytron 810
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylamide | HCID 6579 | — |
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Methylene-bisacrylamide | HCID 53800990 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Lytron 810 | HCID 62707 | — |
反応手順
20 kg. of acrylic acid and 6 kg. of acrylamide are dissolved in 9.5 kg. of distilled water and the acrylic acid is partially neutralized with 12 kg. of KOH. 0.036 kg. of methylenebisacrylamide as a polyvinyl monomer was added as well as 4 kg. of styrene-maleic anhydride resin (3:1 ratio) to provide an aqueous mixed monomer solution. The mixed monomer solution is mixed with 0.28 kg. of 2,2'-azobisisobutyronitrile, dissolved in 2 kg. of acetone as a polymerization initiator. This mixture at a temperature of 60° C. is transferred on an endless belt (600-700 mm. in width, and 7 m. in length) at a thickness of about 1 cm. The polymerization is initiated promptly on the belt resulting in a solid resin.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04820773 |
| 出典データセット | uspto-grants-1989_04 |
| ORD ID | ord-855e9f6bd6014cbeb95d50e28399c647 |
| 出典メモ | uspto-grants-1989_04 |