Dicyclohexylcarbodiimide → HCID 54309069、化合物
反応式
[CH2:1]([C:8]1[CH:9]=[N:10][C:11]([C:14]2[CH:22]=[CH:21][C:17]([C:18]([OH:20])=[O:19])=[CH:16][CH:15]=2)=[N:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[C:23]([C:25]1[CH:30]=[C:29]([CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH3:40])[CH:28]=[CH:27][C:26]=1O)#[N:24].C1(N=C=NC2CCCCC2)CCCCC1>>[CH2:1]([C:8]1[CH:9]=[N:10][C:11]([C:14]2[CH:22]=[CH:21][C:17]([C:18]([O:20][C:26]3[CH:27]=[CH:28][C:29]([CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH3:40])=[CH:30][C:25]=3[C:23]#[N:24])=[O:19])=[CH:16][CH:15]=2)=[N:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]参加物
4
実験手順
29.8 g of 4-(5-heptylpyrimidin-2-yl)-benzoic acid (obtained from 4-(5-heptylpyrimidin-2-yl)-benzonitrile by saponification) and 25.9 g of 2-cyano-4-decylphenol are esterified with one another as described in Example 22 with addition of 21.0 g of dicyclohexylcarbodiimide. 2-Cyano-4-decylphenyl 4-(5-heptylpyrimidin-2-yl)-benzoate is obtained.
出典と根拠
- ORDレコード
- ord-372a9ac66e5140e68af8b4cd141e90a7
- 出典データセット