Potassium Carbonate → HCID 19858315、化合物

HRID 621501ノート

反応式

HRID 621501 の反応式
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

参加物

5

反応物 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

生成物 1

HCID 19858315HCID 19858315、化合物

試薬・触媒・溶媒 1

HCID 24813Phosphorus oxychloride触媒

実験手順

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and concentrated to give the product as an oil.

後処理

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationconcentrated

出典と根拠

ORDレコード
ord-96a9a1d08ed443f8b99ee43952048400
出典データセット
uspto-grants-1989_04
特許番号
US04824849

反応ノート

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